HCID 23132415, compound → 7-Phenylheptan-1-amine

HRID 2097356Notes

Reaction equation

HRID 2097356 reaction equation
[C:1]1([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][N:14]=[N+]=[N-])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1>CCO.[Pd]>[C:1]1([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][NH2:14])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

4

Reactant 1

HCID 23132415HCID 23132415, compound

Product 1

HCID 64319907-Phenylheptan-1-amine

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 702EthanolSolvent2×

Procedure

A solution of 7-phenylheptylazide (3.97 g, 18.3 mmol) in EtOH (15 mL) was added to palladium on carbon (200 mg) in EtOH (35 mL) under an atmosphere of Hydrogen. The mixture was stirred for 24 h at r.t. The mixture was filtered through celite and the solvent was removed under reduced pressure to give the title compound.

Workup

  1. filtrationThe mixture was filtered through celite
  2. customthe solvent was removed under reduced pressure

Sources & evidence

ORD record
ord-b63f1fac05db4c809d4a4b034b60147a
Source dataset
uspto-grants-2013_05
Patent number
US08450348B2

Reaction notes

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