HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23132415, compound → 7-Phenylheptan-1-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23132415 | HCID 23132415 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 7-Phenylheptan-1-amine | HCID 6431990 | — |
Reaction Steps
A solution of 7-phenylheptylazide (3.97 g, 18.3 mmol) in EtOH (15 mL) was added to palladium on carbon (200 mg) in EtOH (35 mL) under an atmosphere of Hydrogen. The mixture was stirred for 24 h at r.t. The mixture was filtered through celite and the solvent was removed under reduced pressure to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08450348B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-b63f1fac05db4c809d4a4b034b60147a |
| Source note | uspto-grants-2013_05 |