HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → 4-[2-(Morpholin-4-yl)ethoxy]phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 4-[2-(Benzyloxy-phenoxy)-ethyl]-morpholine | HCID 2995412 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | 4-[2-(Morpholin-4-yl)ethoxy]phenol | HCID 23132438 | — |
Reaction Steps
A solution of 4-[2-(Benzyloxy-phenoxy)-ethyl]-morpholine (4.77 g, 15.2 mmol) in EtOH (35 mL) was added to palladium on carbon (250 mg) in EtOH (15 mL) under an atmosphere of Hydrogen. The mixture was stirred for 17 h at r.t. The mixture was filtered through celite and the solvent was removed under reduced pressure to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08450348B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-0cc1817318d9413c9b25a1f6249a9104 |
| Source note | uspto-grants-2013_05 |