HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropyl iodide → 4-Bromo-1-methoxy-2-[(propan-2-yl)oxy]benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropyl iodide | HCID 6362 | — |
| Reactant | 5-Bromo-2-methoxyphenol | HCID 142228 | — |
| Product | 4-Bromo-1-methoxy-2-[(propan-2-yl)oxy]benzene | HCID 46738952 | 86% |
Reaction Steps
Reaction and post treatment were carried out in the same manner as in Reference Example 7-(a) except for using 10.1 g (49.8 mmol) of 5-bromo-2-methoxyphenol, and using 15 ml of isopropyl iodide in place of 1-bromo-2-chloroethane, whereby 10.4 g of the title compound was obtained as a pale yellowish solid. (Yield: 86%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08450319B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-a32da5b587a54276a8e4474713d739eb |
| Source note | uspto-grants-2013_05 |