HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66602679, compound → HCID 86627043, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66602679 | HCID 66602679 | — |
| Reactant | HCID 66602907 | HCID 66602907 | — |
| Product | HCID 86627043 | HCID 86627043 | 67% |
Reaction Steps
Reaction and post treatment were carried out in the same manner as in Reference example 24-(g) except for using 5.70 g (10.0 mmol) of 2-bromo-3-bromomethyl-1,5-bis(2-trimethylsilylethoxymethyl)-1,5-dihydropyrrolo[2,3-d]pyridazin-4-one obtained in Reference example 25-(a) in place of 2-bromo-3-bromomethyl-1-(2-trimethylsilylethoxymethyl)-1,5-dihydropyrrolo[2,3-d]pyridazin-4-one, whereby 3.38 g of the title compound was obtained as a white solid. (Yield: 67%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08450319B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-2c65fb10255646389de2cd58983d4f71 |
| Source note | uspto-grants-2013_05 |