HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-bromo-3-(4H-1,2,4-triazol-3-yl)thiophen-2-amine → HCID 56665246, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-bromo-3-(4H-1,2,4-triazol-3-yl)thiophen-2-amine | HCID 59636686 | — |
| Reactant | HCID 68785189 | HCID 68785189 | — |
| Product | HCID 56665246 | HCID 56665246 | — |
Reaction Steps
The title compound was prepared from 2-(2-oxo-7-(trifluoromethyl)-1,6-naphthyridin-1(2H)-yl)acetic acid (55 mg, 0.203 mmol) and 4-bromo-3-(1H-1,2,4-triazol-5-yl)thiophen-2-amine (25 mg, 0.102 mmol) according to protocol A. Retention time (min)=4.505, method [7], MS (ESI) 499.0 (M+H); 1H NMR (300 MHz, CD3OD) δ 9.06 (s, 1H), 8.31 (s, 1H), 8.24 (d, J=9.4 Hz, 1H), 7.94 (s, 1H), 7.14 (s, 1H), 6.99 (d, J=9.4 Hz, 1H), 5.39 (s, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08450363B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-7cb2fde21c8941c1b9e64f8e426b5d74 |
| Source note | uspto-grants-2013_05 |