HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-3-nitrothiophene → 2-Methoxy-4-(3-nitrothiophen-2-yl)thiazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-3-nitrothiophene | HCID 220186 | — |
| Reactant | 2-Methoxy-4-(tributylstannyl)thiazole | HCID 2763264 | — |
| Product | 2-Methoxy-4-(3-nitrothiophen-2-yl)thiazole | HCID 68755761 | — |
Reaction Steps
2-Methoxy-4-(3-nitrothiophen-2-yl)thiazole was prepared from 2-methoxy-4-(tributylstannyl)thiazole (1.0 g, 2.47 mmol) and 2-chloro-3-nitrothiophene (0.404 g, 2.47 mmol) according to protocol E. Retention time (min)=2.516, method [1], MS (ESI) 242.9 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08450363B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-cd16429c3f3b4f1f81e013a38e4920a2 |
| Source note | uspto-grants-2013_05 |