反应详情

To a stirred solution of T10.6 (0.035 g, 0.10 mmol) in DCM (2.00 mL) and DMF (0.01 mL) at 0° C. was added thionyl chloride (0.01 g, 0.10 mmol). The reaction was then stirred at room temperature for 2 hours and was then concentrated in vacuo. The resulting product was then purified on silica gel (0-10% EtOAc in hexanes) to yield T10 as a colorless oil (0.035 g, 95% yield).

1. concentrationwas then concentrated in vacuo
2. customThe resulting product was then purified on silica gel (0-10% EtOAc in hexanes)