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HRID2099343

反应详情

EQUATION

反应方程式

HRID 2099343 的结构方程式

REACTANTS

反应物

2
结构：COCCS(N)(F)(F)(F)CCOC
HCID53904438

未命名化合物

结构：CN1[C@@H]2CC=C[C@@]1(OC(=O)C(O)(c1ccc(F)cc1)c1ccc(F)cc1)CC2
HCID86585677

未命名化合物

PRODUCTS

生成物

1
结构：CN1[C@@H]2CC=C[C@@]1(O)CC2.O=C([O-])C(F)(c1ccc(F)cc1)c1ccc(F)cc1
HCID86585678

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

2.94 g (0.013 mol) of bis-(2-methoxyethyl)-aminosulfur trifluoride are reacted with 3.85 g (0.01 mol) of 5d analogously to Example 4, step 4.3 in 100 mL of dichloromethane. The product is recrystallized from acetonitrile in the form of its hydrochloride. Yield: 2.93 g (69% of theory).

WORKUP

后处理

  1. customThe product is recrystallized from acetonitrile in the form of its hydrochloride