HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53904438, compound → HCID 86585678, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53904438 | HCID 53904438 | — |
| Reactant | Tropenol 4,4'-difluorobenzilate | HCID 86585677 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86585678 | HCID 86585678 | — |
Reaction Steps
2.94 g (0.013 mol) of bis-(2-methoxyethyl)-aminosulfur trifluoride are reacted with 3.85 g (0.01 mol) of 5d analogously to Example 4, step 4.3 in 100 mL of dichloromethane. The product is recrystallized from acetonitrile in the form of its hydrochloride. Yield: 2.93 g (69% of theory).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07569581B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-370f8c352a01470fa6ebc33e5e62d449 |
| Source note | uspto-grants-2009_08 |