HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59442734, compound → 3-Amino-N-methyl-5-(trifluoromethyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59442734 | HCID 59442734 | — |
| Reactant | HCID 59631038 | HCID 59631038 | — |
| Product | 3-Amino-N-methyl-5-(trifluoromethyl)benzamide | HCID 57431453 | — |
Reaction Steps
Utilising the procedure described in Example 86e, but employing α,α,α-trifluoro-N-methyl-5-nitro-m-toluamide (Dean E. Welch, J. Med. Chem. (1969), 12, 299-303) in lieu of 3-(4-morpholinyl)-5-nitro-N-(methyl)-benzamide, afforded the title compound as a beige crystalline solid, m.p. 113-115° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07569566B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-5d650ab6dcb34828b0ea01ddd2a87c8d |
| Source note | uspto-grants-2009_08 |