Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 22285186 | HCID 22285186 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 22285184 | HCID 22285184 | — |
Reaction Steps
A catalytic amount of concentrated sulfuric acid was added dropwise to an acetic anhydride (55 ml) suspension of 5-(4′-methoxyphenyl)-2-nitroaniline (2.02 g), followed by 3 hours and 20 minutes stirring at 40° C. After cooling to room temperature, diethyl ether (200 ml) was added thereto and the precipitated powder was collected by filtration to obtain N-(4′-methoxy-4-nitrobiphenyl-3-yl)acetamide (596 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07569688B2 |
|---|
| Source dataset | uspto-grants-2009_08 |
|---|
| ORD ID | ord-c02e0a59307548da865b3627ee7e6a72 |
|---|
| Source note | uspto-grants-2009_08 |
|---|
