HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 69054704, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 57796667 | HCID 57796667 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 69054704 | HCID 69054704 | 95% |
Reaction Steps
10 mg (0.02 mmol) of tert-butyl 5-[6-benzoylamino-1-(3-methylbut-2-enyl)-1H-benzimidazol-2-yl]hexahydropyrrolo[3,4-c]pyrrole-2-carboxylate were dissolved in 200 μl of trifluoroacetic acid and 200 μl of water, and stirred at room temperature for 19 hours. The reaction mixture was diluted with water and freeze-dried. 10 mg (95%) of the desired product were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07569700B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-935edd1aee744b51b2654df0856e5533 |
| Source note | uspto-grants-2009_08 |