HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl isocyanate → HCID 135899126, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl isocyanate | HCID 76639 | — |
| Reactant | HCID 136312202 | HCID 136312202 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 135899126 | HCID 135899126 | — |
Reaction Steps
Benzyl isocyanate was added to a solution of 2-aminomethyl-3H-pyrido[2,3-d]pyrimidin-4-one (example 24.1) in pyridine; the reaction mixture was kept at r.t. overnight. The volatiles were evaporated and the title compound was isolated from the reaction mixture by reversed-phase, preparative HPLC. MS: m/e=308.4 [M−H−].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07572801B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-02b36d586a0e454a862246137c1e779d |
| Source note | uspto-grants-2009_08 |