HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Difluoropyridine-3-carboxylic acid → HCID 135899206, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Difluoropyridine-3-carboxylic acid | HCID 10583070 | — |
| Reactant | HCID 67100781 | HCID 67100781 | — |
| Product | HCID 135899206 | HCID 135899206 | 80% |
Reaction Steps
The title compound was synthesized in analogy to example 85 using 2,6-difluoropyridine-3-carboxylic acid and 2-[2-(2-fluorophenyl)-ethoxy]-acetamidine to give 7-fluoro-2-[2-(2-fluorophenyl)-ethoxymethyl]-3H-pyrido[2,3-d]pyrimidin-4-one as the desired product (80%) as a white solid. MS: m/e=318.2 [M+H+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07572801B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-9057f8e618c64378bff652427f8ce355 |
| Source note | uspto-grants-2009_08 |