HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Phenyl-1-pentanol → HCID 136368384, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Phenyl-1-pentanol | HCID 61523 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Reactant | HCID 136345808 | HCID 136345808 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 136368384 | HCID 136368384 | — |
Reaction Steps
In analogy to the procedure described in example 97.3, 2-chloro-7-methyl-3H-pyrido[2,3-d]pyrimidin-4-one hydrochloride was reacted with 5-phenyl-1-pentanol in DMSO in the presence of molecular sieves and potassium tert-butylate to give 7-methyl-2-(5-phenyl-pentyloxy)-3H-pyrido[2,3-d]pyrimidin-4-one as yellow crystals. MS: m/e=324.4 [M+H+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07572801B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-f8d54e9506244d9889e20a2fd8da950f |
| Source note | uspto-grants-2009_08 |