HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium tert-butoxide → HCID 136368389, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Reactant | HCID 140520074 | HCID 140520074 | — |
| Product | HCID 136368389 | HCID 136368389 | — |
Reaction Steps
In analogy to the procedure described in example 78.4, 2,5-dichloro-N-[5-(4-fluoro-phenyl)-1-imino-pentyl]-nicotinamide was treated with KOtBu to obtain 6-chloro-2-[4-(4-fluoro-phenyl)-butyl]-3H-pyrido[2,3-d]pyrimidin-4-one as off-white crystals. MS: m/e=332.2 [M+H+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07572801B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-5c6b3ace4afc4184a9970bdc56a5768b |
| Source note | uspto-grants-2009_08 |