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HRID2100543

反应详情

EQUATION

反应方程式

HRID 2100543 的结构方程式

REACTANTS

反应物

4
结构：CCN(C(C)C)C(C)C
HCID81531

Diisopropylethylamine

C8H19N

结构：CN(C)C(On1nnc2ccccc21)=[N+](C)C.F[B-](F)(F)F
HCID2733207

O-(Benzotriazol-1-yl)-N,N,N′,N′-tetramethyluronium tetrafluoroborate

C11H16BF4N5O

结构：O=C(O)c1cc(Cl)cnc1Cl
HCID2736085

2,5-Dichloronicotinic acid

C6H3Cl2NO2

结构：Cl.N=C(N)COCCc1ccc2ccccc2c1
HCID67099300

未命名化合物

PRODUCTS

生成物

1
结构：N=C(COCCc1ccc2ccccc2c1)NC(=O)c1cc(Cl)cnc1Cl
HCID140520068

未命名化合物

PROCEDURE

实验过程

In analogy to the procedure described in example 78.3, 2,5-dichloronicotinic acid was reacted with 2-(2-naphthalen-2-yl-ethoxy)-acetamidine hydrochloride in the presence of TBTU and DIPEA to give 2,5-dichloro-N-[1-imino-2-(2-naphthalen-2-yl-ethoxy)-ethyl]-nicotinamide as yellow oil. MS: m/e=402.3 [M+H+].