huagongshe.com
HRID2100554

反应详情

EQUATION

反应方程式

HRID 2100554 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)[O-].[K+]
HCID23665647

2-Methyl-2-propanol, potassium salt

C4H9KO

结构：CCCCc1cnc(Cl)c(C(=O)NC(=N)COCCc2cccc(Cl)c2)c1
HCID140520071

未命名化合物

PRODUCTS

生成物

1
结构：CCCCc1cnc2nc(COCCc3cccc(Cl)c3)[nH]c(=O)c2c1
HCID136368400

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CS(C)=O
溶剂HCID679

Dimethyl sulfoxide

C2H6OS

PROCEDURE

实验过程

In analogy to the procedure described in example 78.4, 5-butyl-2-chloro-N-{2-[2-(3-chloro-phenyl)-ethoxy]-1-imino-ethyl}-nicotinamide was treated with KOtBu in DMSO to obtain 6-butyl-2-[2-(3-chloro-phenyl)-ethoxymethyl]-3H-pyrido[2,3-d]pyrimidin-4-one as off-white crystals. MS: m/e=370.4 [M−H−].