HCID 57799784, compound → HCID 57799551, compound

HRID 2101092Notes

Reaction equation

HRID 2101092 reaction equation
Cl[C:2]1[N:3]=[C:4]([NH:16][C:17]2[CH:21]=[C:20]([CH3:22])[NH:19][N:18]=2)[CH:5]=[C:6]2[C:15]=1[CH:14]=[CH:13][C:12]1[O:11][CH2:10][CH2:9][O:8][C:7]2=1>CC(O)C>[CH:7]([O:8][C:2]1[N:3]=[C:4]([NH:16][C:17]2[CH:21]=[C:20]([CH3:22])[NH:19][N:18]=2)[CH:5]=[C:6]2[C:15]=1[CH:14]=[CH:13][C:12]1[O:11][CH2:10][CH2:9][O:8][C:7]2=1)([CH3:12])[CH3:6]

Participants

3

Reactant 1

HCID 57799784HCID 57799784, compound

Product 1

HCID 57799551HCID 57799551, compound

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent

Procedure

Similar procedure as described in example 10 was used, starting from (8-Chloro-2,3-dihydro-1,4-dioxa-7-aza-phenanthren-6-yl)-(5-methyl-1H-pyrazol-3-yl)-amine and 2-propanol to give (8-Isopropoxy-2,3-dihydro-1,4-dioxa-7-aza-phenanthren-6-yl)-(5-methyl-1H-pyrazol-3-yl)-amine. LC-MS m/e 341(MH+).

Sources & evidence

ORD record
ord-8bd06f2da00a4089ae887f34ee77aa95
Source dataset
uspto-grants-2009_08
Patent number
US07572809B2

Reaction notes

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