1H-Pyrazol-3-amine, 5-methyl- → HCID 57799646, compound

Participants

Reaction Conditions

Reaction Steps

A 10˜20 mL process vial was charged with 500 mg 2-Cyanomethyl-4-methoxy-3-methyl-benzoic acid and 5-Methyl-1H-pyrazol-3-ylamine in 15 mL AcOH. The vial was heated at 130° C. for 30 min under microwave irradiation. Most of the solvent was removed under reduced pressure, and the residue was poured into ice-water. The solid was collected and washed with water.

Provenance & Evidence