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HRID2101139

反应详情

EQUATION

反应方程式

HRID 2101139 的结构方程式

REACTANTS

反应物

2
结构：O=P(Cl)(Cl)Cl
HCID24813

Phosphoric trichloride

Cl3OP

结构：COc1cc2c(O)nc(Nc3cc(C)[nH]n3)cc2c(Cl)c1OC
HCID178486774

未命名化合物

PRODUCTS

生成物

1
结构：COc1cc2c(Cl)nc(Nc3cc(C)[nH]n3)cc2c(Cl)c1OC
HCID57799846

未命名化合物

PROCEDURE

实验过程

Similar procedure as described in example 9B was used, starting from 5-Chloro-6,7-dimethoxy-3-(5-methyl-1H-pyrazol-3-ylamino)-isoquinolin-1-ol and POCl3 to give (1,5-Dichloro-6,7-dimethoxy-isoquinolin-3-yl)-(5-methyl-1H-pyrazol-3-yl)-amine. LC-MS: m/e 353 (MH+).