Butyl nitrite → HCID 76608754, compound

HRID 2101141Notes

Reaction equation

[Br:1][C:2]1[CH:3]=[C:4]2[C:8](=[CH:9][CH:10]=1)[C:7](=[O:11])[CH2:6][CH2:5]2.C([O:16][N:17]=O)CCC>>[Br:1][C:2]1[CH:3]=[C:4]2[C:8](=[CH:9][CH:10]=1)[C:7](=[O:11])[C:6](=[N:17][OH:16])[CH2:5]2

Participants

Reactant 2

HCID 10996Butyl nitrite

HCID 5206955-Bromo-1-indanone

Product 1

HCID 76608754HCID 76608754, compound

Procedure

Similar procedure as described in example 9B was used, starting from 5-Bromo-indan-1-one and n-butylnitrite to give 5-Bromo-indan-1,2-dione 2-oxime. LC-MS: m/e 240 (MH+).

Sources & evidence

ORD record: ord-88c7e56dbe964e04a0bfdce08931ce63
Source dataset: uspto-grants-2009_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07572809B2

Reaction notes

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