HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Toluenesulfonyl chloride → 5-Bromo-2-(cyanomethyl)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| Reactant | 6-Bromo-indan-1,2-dione 2-oxime | HCID 76608743 | — |
| Product | 5-Bromo-2-(cyanomethyl)benzoic acid | HCID 57799748 | — |
Reaction Steps
Similar procedure as described in example 9B was used, starting from 6-Bromo-indan-1,2-dione 2-oxime and p-Toluenesulfonyl chloride to give 5-Bromo-2-cyanomethyl-benzoic acid. LC-MS: m/e: 238 (M−1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07572809B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-9bb8b35719054e0a930986f4764314ab |
| Source note | uspto-grants-2009_08 |