HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Fluorophenethylamine → [2-(4-Fluoro-phenyl)-ethyl]-(4-trimethylsilanyl-benzyl)-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Fluorophenethylamine | HCID 4653 | — |
| Reactant | 4-(Trimethylsilyl)benzaldehyde | HCID 637573 | — |
| Product | [2-(4-Fluoro-phenyl)-ethyl]-(4-trimethylsilanyl-benzyl)-amine | HCID 57438507 | — |
Reaction Steps
[2-(4-fluoro-phenyl)-ethyl]-(4-trimethylsilanyl-benzyl)-amine was prepared in analogy to example 1 from 4-trimethylsilanyl-benzaldehyde and 2-(4-fluoro-phenyl)-ethylamine. MS (ISP): 302.2 (100) (M+H)+. 1H NMR (CDCl3, 300 MHz): δ 7.47 (d, 2H), 7.27 (d, 2H), 7.15 (dd, 2H), 6.97 (dt, 2H) 3.79 (s, 2H), 2.75-3.00 (m, 4H), 0.26 (s, 9H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07572823B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-97c9275eebd0421684e5020ca4098fd6 |
| Source note | uspto-grants-2009_08 |