Tert-Butylamine → HCID 9925135, compound

HRID 2101698Notes

Reaction equation

HRID 2101698 reaction equation
[C:1]([NH2:5])([CH3:4])([CH3:3])[CH3:2].[CH3:6][C:7]1[CH:12]=[CH:11][C:10]([C:13]2[N:14]=[C:15]([C:26](O)=[O:27])[N:16]([CH3:25])[C:17]=2[C:18]2[CH:23]=[CH:22][C:21]([CH3:24])=[CH:20][CH:19]=2)=[CH:9][CH:8]=1>>[C:1]([NH:5][C:26]([C:15]1[N:16]([CH3:25])[C:17]([C:18]2[CH:23]=[CH:22][C:21]([CH3:24])=[CH:20][CH:19]=2)=[C:13]([C:10]2[CH:9]=[CH:8][C:7]([CH3:6])=[CH:12][CH:11]=2)[N:14]=1)=[O:27])([CH3:4])([CH3:3])[CH3:2]

Participants

3

Reactant 2

HCID 6385Tert-ButylamineHCID 22066080HCID 22066080, compound

Product 1

HCID 9925135HCID 9925135, compound

Procedure

Using essentially the same procedure as Example 9, Step B, but using t-butylamine (0.022 mL), 4,5-di-(4-methylphenyl)-1-methylimidazole-2-carboxylic acid (25 mg, 0.08 mmol) from Example 9, Step A was converted to the title compound.

Sources & evidence

ORD record
ord-0a9c4b3eeb00450b91b32dcf863751dd
Source dataset
uspto-grants-2009_08
Patent number
US07572785B2

Reaction notes

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