Ammonia → HCID 9970059, compound

HRID 2101742Notes

Reaction equation

HRID 2101742 reaction equation
[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[C:9]1[N:10]=[C:11]([C:22]([O:24]CC)=O)[N:12]([CH3:21])[C:13]=1[C:14]1[CH:19]=[CH:18][C:17]([Cl:20])=[CH:16][CH:15]=1.[NH3:27]>CO>[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[C:9]1[N:10]=[C:11]([C:22]([NH2:27])=[O:24])[N:12]([CH3:21])[C:13]=1[C:14]1[CH:19]=[CH:18][C:17]([Cl:20])=[CH:16][CH:15]=1

Participants

4

Reactant 2

HCID 222AmmoniaHCID 10179718HCID 10179718, compound

Product 1

HCID 9970059HCID 9970059, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The title compound was prepared from ethyl 4-(2,4-dichlorophenyl)-5-(4-chlorophenyl)-1-methylimidazole-2-carboxylate and 2 M NH3 in MeOH following the method of example 36, step B (method B). LC-MS: Rt=3.6 min. m/e=379.9 (M+1).

Sources & evidence

ORD record
ord-5904912046b64b72b102ce2dd109a980
Source dataset
uspto-grants-2009_08
Patent number
US07572785B2

Reaction notes

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