Tributylamine → HCID 22596642, compound

HRID 2102253Notes

Reaction equation

[CH2:1]([N:5]([CH2:10][CH2:11][CH2:12][CH3:13])[CH2:6][CH2:7][CH2:8][CH3:9])[CH2:2][CH2:3][CH3:4].[C:14]([O-:18])(=[O:17])[CH:15]=[CH2:16]>>[C:14]([O-:18])(=[O:17])[CH:15]=[CH2:16].[CH2:10]([N:5]([CH2:1][CH2:2][CH2:3][CH3:4])[CH2:6][CH2:7][CH2:8][CH3:9])[CH2:11][CH2:12][CH3:13]

Participants

Reactant 2

HCID 7622Tributylamine

HCID 25188Acrylate

Product 1

HCID 22596642HCID 22596642, compound

Procedure

150 mg tributylamine was added to 1.16 g of the “acrylate component” and mixed until homogeneity to form the “acrylate/tributylamine component”. Subsequently, 1.5 g of the “thiol component” was mixed with the “acrylate/tributylamine component” until homogeneity was achieved.

Workup

additionmixed until homogeneity

Sources & evidence

ORD record: ord-54cd0954d7914ed4a8439d82b93e0b35
Source dataset: uspto-grants-2009_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07575740B2

Reaction notes

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