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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2102318Generated: October 31, 2026

Dichloromethane → HCID 66970990, compound

https://huagongshe.com/reaction/2102318

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDichloromethaneHCID 6344—
ReactantHCID 66971319HCID 66971319—
CatalystHCID 178418390HCID 178418390—
SolventEthanolHCID 702—
ProductHCID 66970990HCID 6697099089.9%

Reaction Steps

To a solution of [3-benzyloxy-1-isopropyl-5-(4-methoxyphenyl)-1H-pyrazol-4-yl]4-methoxy-phenyl methanol (0.11 g) in ethanol (4 mL) was added a catalytic amount of 10% palladium-carbon powder and the mixture was stirred at room temperature under a hydrogen atmosphere overnight. Dichloromethane was added to the mixture and the insoluble material was removed by filtration. The solvent of filtrate was removed under reduced pressure to give the title compound (0.076 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07576063B2
Source datasetuspto-grants-2009_08
ORD IDord-69e7d50d58da4a2aa265435aa5ffaf47
Source noteuspto-grants-2009_08