HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → HCID 57803105, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | 8-Chloro-2-(3-methoxyphenyl)imidazo[1,2-a]pyrazine | HCID 57803134 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 57803105 | HCID 57803105 | — |
Reaction Steps
To the product from example 170 in acetic acid (10 mL) was added a solution of bromine in acetic acid (0.25 mmol, 1 mL). Concentration of the reaction mixture afforded crude 3-bromo-8-chloro-2-(3-methoxy-phenyl)-imidazo[1,2-a]pyrazine. MH+ (LCMS) 338.0(m/z).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07576085B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-8a85253990a34709980ac78506dab0db |
| Source note | uspto-grants-2009_08 |