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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2102641Generated: October 30, 2026

Sodium Iodide → HCID 68908797, compound

https://huagongshe.com/reaction/2102641

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium IodideHCID 5238—
ReactantDimethylformamideHCID 6228—
ReactantPotassium CarbonateHCID 11430—
Reactant3-Pentyl-8-azabicyclo[3.2.1]octaneHCID 21989852—
ProductHCID 68908797HCID 68908797—

Reaction Steps

Crude (R,S)-1-(3-chloro-2-methylpropyl)-3,4-dihydro-1H-quinolin-2-one (107LH63) (0.094 g), 3-pentyl-8-azabicyclo[3.2.1]octane (0.027 g, 0.15 mmol), NaI (0.100 g, 0.67 mmol), and K2CO3 (0.075 g, 0.54 mmol) in DMF (1 mL) were reacted and purified according to GP20 to give the title compound (107LH74-c5) (0.023 g). HPLC-MS (ammonium acetate) [M+H]+=383.34.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07576078B2
Source datasetuspto-grants-2009_08
ORD IDord-844924033ac642fc8bff035a60fd1791
Source noteuspto-grants-2009_08