Sodium Hydroxide → HCID 57804160, compound

Participants

Reaction Conditions

Reaction Steps

Methyl 2-fluoro-3-methoxy-4-(3,3-dimethylbut-1-ynyl)benzoate (760 mg, 2.7 mmol) was dissolved in MeOH (10 mL), NaOH (in 10 mL water) was added and stirred at 50° C. for 1 h. Solvent was removed, more water was added, neutralized by HCl till pH˜2, white solid thus formed was filtered out, dried in vacuum oven (at 65° C.). Product was obtained as a white solid (760 mg, 93%).

Provenance & Evidence