HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68703275, compound → (7-Aminoquinolin-3-yl)methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68703275 | HCID 68703275 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | (7-Aminoquinolin-3-yl)methanol | HCID 59020657 | — |
Reaction Steps
A mixture of benzyl 3-(hydroxymethyl)quinolin-7-ylcarbamate (480 mg, 0.0016 mol), 10% Pd-C (50 mg), and MeOH (50 mL) was stirred under H2 (1 atm) for 1 h. The catalyst was filtered-off and the filtrate was concentrated to give the product as a yellow solid. LC-MS: 0.34 min, 175.1 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07576099B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-e762c4d1547747cf8c266e8ca536ca4e |
| Source note | uspto-grants-2009_08 |