Dichloromethane → 8-bromo-1,4-dioxaspiro[4.5]decane

HRID 210301Notes

Reaction equation

HRID 210301 reaction equation
[C:12]([Br:13])([Br:14])([Br:15])[Br:16].[CH2:36]([Cl:37])[Cl:38].[O:1]1[CH2:2][CH2:3][O:4][C:5]12[CH2:6][CH2:7][CH:8]([OH:11])[CH2:9][CH2:10]2.[c:17]1([P:18]([c:19]2[cH:20][cH:21][cH:22][cH:23][cH:24]2)[c:25]2[cH:26][cH:27][cH:28][cH:29][cH:30]2)[cH:31][cH:32][cH:33][cH:34][cH:35]1>>[O:1]1[CH2:2][CH2:3][O:4][C:5]12[CH2:6][CH2:7][CH:8]([Br:13])[CH2:9][CH2:10]2

Participants

5

Reactant 4

HCID 6344DichloromethaneHCID 11205Carbon tetrabromideHCID 11776TriphenylphosphineHCID 5673521,4-Dioxaspiro(4.5)decan-8-ol

Product 1

HCID 137651298-bromo-1,4-dioxaspiro[4.5]decane

Sources & evidence

ORD record
ord-59ce7d7dacbe49b1bae6278fba862604
Source dataset
Training data from https://doi.org/10.1039/C8SC04228D (6/10)

Reaction notes

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