HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 69055644, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 69054367 | HCID 69054367 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 69055644 | HCID 69055644 | — |
Reaction Steps
To a solution of 6-hydroxy-5,7-dimethylspiro[chromene-2,1′-cyclobutan]-4(3H)-one,( 345 mg) in methanol (5 mL) was added sodium borohydride (65 mg). The mixture was stirred at room temperature for 30 min. The mixture was concentrated and the methanol removed to give 5,7-dimethyl-3,4-dihydrospiro[chromene-2,1′-cyclobutane]-4,6-diol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07576094B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-c5a29e90eb9643d18d0e8107b8db69f8 |
| Source note | uspto-grants-2009_08 |