Benzophenone → HCID 22475011, compound

HRID 2103104Notes

Reaction equation

HRID 2103104 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8](F)(F)F)=[CH:4][CH:3]=1.[Al+3].[Cl-:13].[Cl-:14].[Cl-].[C:16]1([O:22][CH3:23])[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1.C(C1C=CC=CC=1)(=O)C1C=CC=CC=1>>[CH3:23][O:22][C:16]1[CH:21]=[CH:20][C:19]([C:8]([C:5]2[CH:6]=[CH:7][C:2]([Cl:1])=[CH:3][CH:4]=2)([Cl:14])[Cl:13])=[CH:18][CH:17]=1

Participants

5

Reactant 4

HCID 3102BenzophenoneHCID 73941-Chloro-4-(trifluoromethyl)benzeneHCID 7519AnisoleHCID 6451240Aluminum(III) Chloride

Product 1

HCID 22475011HCID 22475011, compound

Procedure

From 4-chlorobenzotrifluoride (180 mg, 1 mmol), AlCl3 (400 mg, 3 mmol) and anisole (108 mg, 1 mmol), red solid (345 mg, 120% crude), contains the benzophenone (ca 30%).

Sources & evidence

ORD record
ord-12a42533cba9420d893e73d8ae6a50fc
Source dataset
uspto-grants-2009_08
Patent number
US07576088B2

Reaction notes

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