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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2103684Generated: October 31, 2026

HCID 178452023, compound → HCID 178494068, compound

https://huagongshe.com/reaction/2103684

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 178452023HCID 178452023—
ReactantHCID 178494069HCID 178494069—
ProductHCID 178494068HCID 178494068—

Reaction Steps

The title compound was prepared according to the procedure described in Example 38C, substituting the product of Example 39A for the product of Example 38B. 1H NMR (500 MHz, CDCl3) δ ppm 8.77 (s, 2H) 8.05 (d, J=8.54 Hz, 1H) 7.97 (s, 1H) 7.58 (dd, J=8.54, 1.83 Hz, 1H) 4.08 (s, 3H) 3.85-3.98 (m, 1H) 3.60-3.70 (m, 1H) 3.08-3.16 (m, 1H) 2.90-3.02 (m, 2H) 2.73-2.81 (m, 1H) 2.61-2.71 (m, 2H) 2.49-2.60 (m, 3H) 2.31-2.47 (m, 3H) 1.93-2.05 (m, 1H) 1.58-1.74 (m, 1H). MS: (M+H)+=408.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07576110B2
Source datasetuspto-grants-2009_08
ORD IDord-42566abd3244412eaea1d4651f823cb4
Source noteuspto-grants-2009_08