HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178452023, compound → HCID 178494068, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178452023 | HCID 178452023 | — |
| Reactant | HCID 178494069 | HCID 178494069 | — |
| Product | HCID 178494068 | HCID 178494068 | — |
Reaction Steps
The title compound was prepared according to the procedure described in Example 38C, substituting the product of Example 39A for the product of Example 38B. 1H NMR (500 MHz, CDCl3) δ ppm 8.77 (s, 2H) 8.05 (d, J=8.54 Hz, 1H) 7.97 (s, 1H) 7.58 (dd, J=8.54, 1.83 Hz, 1H) 4.08 (s, 3H) 3.85-3.98 (m, 1H) 3.60-3.70 (m, 1H) 3.08-3.16 (m, 1H) 2.90-3.02 (m, 2H) 2.73-2.81 (m, 1H) 2.61-2.71 (m, 2H) 2.49-2.60 (m, 3H) 2.31-2.47 (m, 3H) 1.93-2.05 (m, 1H) 1.58-1.74 (m, 1H). MS: (M+H)+=408.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07576110B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-42566abd3244412eaea1d4651f823cb4 |
| Source note | uspto-grants-2009_08 |