HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1,1-Trifluoro-2,4-pentanedione → HCID 11710932, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1,1-Trifluoro-2,4-pentanedione | HCID 73943 | — |
| Reactant | 2-Amino-5-bromobenzophenone | HCID 99677 | — |
| Solvent | Ethylacetate heptane | HCID 21899848 | — |
| Product | HCID 11710932 | HCID 11710932 | 50% |
Reaction Steps
The title compound was prepared from (2-Amino-5-bromo-phenyl)-phenyl-methanone [example A16] and 1,1,1-trifluoro-2,4-pentanedione according to the procedure of example 1, except that heptane/ethyl acetate (10:1) was used. Yield: 50%; MS: m/z=392/394 (M).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07576217B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-61fbbd4bd1c0492781fb2a19637495ed |
| Source note | uspto-grants-2009_08 |