HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetylacetone → HCID 11509149, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetylacetone | HCID 31261 | — |
| Reactant | HCID 68405958 | HCID 68405958 | — |
| Solvent | Ethylacetate heptane | HCID 21899848 | — |
| Product | HCID 11509149 | HCID 11509149 | 61% |
Reaction Steps
The title compound was prepared from (2-Amino-5-trifluoromethoxy-phenyl)-(4-chloro-phenyl)-methanone [example A3] and acetylacetone according to the method of example 1, except that heptane/ethyl acetate (1:2) was used. Yield: 61%. MS: m/z=379 (M).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07576217B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-287e679406e24819ac0a8608bef8b150 |
| Source note | uspto-grants-2009_08 |