Acetylacetone → HCID 11517213, compound

HRID 2104148Notes

Reaction equation

HRID 2104148 reaction equation
[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([O:8][C:9]([F:12])([F:11])[F:10])=[CH:4][C:3]=1[C:13]([C:15]1[CH:20]=[CH:19][C:18]([Cl:21])=[C:17]([Cl:22])[CH:16]=1)=O.[C:23]([CH2:26][C:27](=O)[CH3:28])(=[O:25])[CH3:24]>CCCCCCC.C(OCC)(=O)C>[Cl:22][C:17]1[CH:16]=[C:15]([C:13]2[C:3]3[C:2](=[CH:7][CH:6]=[C:5]([O:8][C:9]([F:12])([F:11])[F:10])[CH:4]=3)[N:1]=[C:27]([CH3:28])[C:26]=2[C:23](=[O:25])[CH3:24])[CH:20]=[CH:19][C:18]=1[Cl:21]

Participants

4

Reactant 2

HCID 31261AcetylacetoneHCID 67548725HCID 67548725, compound

Product 1

HCID 11517213HCID 11517213, compoundYield 59%

Reagents, catalysts & solvents 1

HCID 21899848Ethylacetate heptaneSolvent

Procedure

The title compound was prepared from (2-Amino-5-trifluoromethoxy-phenyl)-(3,4-dichloro-phenyl)-methanone [example A4] and acetylacetone according to the method of example 1, except that heptane/ethyl acetate (1:2). Yield: 59%. MS: m/z=414 (M).

Sources & evidence

ORD record
ord-61232eb994ca46b79d56f618512330b9
Source dataset
uspto-grants-2009_08
Patent number
US07576217B2

Reaction notes

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