HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetylacetone → HCID 11517213, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetylacetone | HCID 31261 | — |
| Reactant | HCID 67548725 | HCID 67548725 | — |
| Solvent | Ethylacetate heptane | HCID 21899848 | — |
| Product | HCID 11517213 | HCID 11517213 | 59% |
Reaction Steps
The title compound was prepared from (2-Amino-5-trifluoromethoxy-phenyl)-(3,4-dichloro-phenyl)-methanone [example A4] and acetylacetone according to the method of example 1, except that heptane/ethyl acetate (1:2). Yield: 59%. MS: m/z=414 (M).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07576217B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-61232eb994ca46b79d56f618512330b9 |
| Source note | uspto-grants-2009_08 |