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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2104149Generated: October 30, 2026

Acetylacetone → HCID 11494785, compound

https://huagongshe.com/reaction/2104149

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetylacetoneHCID 31261—
ReactantHCID 67549273HCID 67549273—
SolventIsopropanolHCID 3776—
ProductHCID 11494785HCID 1149478542%

Reaction Steps

The title compound was prepared from (2-Amino-5-phenoxy-phenyl)-(4-chloro-phenyl)-methanone [example A5] and acetylacetone according to the method of example 1, except that the solvent was isopropanol, the reaction time was of 16.5 h and the residue was purified by spontaneous crystallization from the reaction mixture. Yield: 42%; MS: m/z=387 (M).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07576217B2
Source datasetuspto-grants-2009_08
ORD IDord-2485ccc67a9248d2936c696d87677569
Source noteuspto-grants-2009_08