HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetylacetone → HCID 11494785, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetylacetone | HCID 31261 | — |
| Reactant | HCID 67549273 | HCID 67549273 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 11494785 | HCID 11494785 | 42% |
Reaction Steps
The title compound was prepared from (2-Amino-5-phenoxy-phenyl)-(4-chloro-phenyl)-methanone [example A5] and acetylacetone according to the method of example 1, except that the solvent was isopropanol, the reaction time was of 16.5 h and the residue was purified by spontaneous crystallization from the reaction mixture. Yield: 42%; MS: m/z=387 (M).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07576217B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-2485ccc67a9248d2936c696d87677569 |
| Source note | uspto-grants-2009_08 |