HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → HCID 11590020, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | 1,1,1-Trifluoro-2,4-pentanedione | HCID 73943 | — |
| Reactant | HCID 67549818 | HCID 67549818 | — |
| Solvent | Ethylacetate heptane | HCID 21899848 | — |
| Product | HCID 11590020 | HCID 11590020 | 58% |
Reaction Steps
The title compound was prepared from (2-Amino-5-trifluoromethoxy-phenyl)-(4-methoxy-phenyl)-methanone [example A8] and 1,1,1-trifluoro-2,4-pentanedione according to the procedure of example 1, except that the solvent was isopropanol, the reaction time was of 17 h and a grandient of heptane/ethyl acetate was used. Yield: 58%; MS: m/z=429 (M).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07576217B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-8a921723abd740dda3ece776547f9f64 |
| Source note | uspto-grants-2009_08 |