HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azepane → HCID 11618848, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azepane | HCID 8119 | — |
| Reactant | HCID 11567771 | HCID 11567771 | — |
| Product | HCID 11618848 | HCID 11618848 | 32% |
Reaction Steps
The title compound was prepared from 1-[6-Bromo-4-(4-fluoro-phenyl)-2-methyl-quinolin-3-yl]-2,2,2-trifluoro-ethanone [example 24] and azepane according to the procedure of example 25, except that the reaction time was of 16 h. Yield: 32%; MS: m/z=431 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07576217B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-f685ff4631de49229cb5cb2ff5272ec7 |
| Source note | uspto-grants-2009_08 |