HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → HCID 11704924, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | 1-Cyclopropyl-butane-1,3-dione | HCID 11018869 | — |
| Reactant | HCID 68405963 | HCID 68405963 | — |
| Solvent | Ethylacetate heptane | HCID 21899848 | — |
| Product | HCID 11704924 | HCID 11704924 | 47% |
Reaction Steps
The title compound was prepared from (2-Amino-5-bromo-phenyl)-(4-methanesulfonyl-phenyl)-methanone [example A15] and 1-cyclopropyl-1,3-butanedione according to the procedure of example 1, except that the solvent was isopropanol, the reaction time was of 16 h and heptane/ethyl acetate (1:2) was used. Yield: 47%; MS: m/z=443 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07576217B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-bc7a2e69056e42b3ade1cb1c7499aac2 |
| Source note | uspto-grants-2009_08 |