Benzyl Bromide → HCID 18765779, compound

HRID 2104297Notes

Reaction equation

HRID 2104297 reaction equation
[ClH:1].[NH2:2][C:3](=[N:9][C:10]1[CH:11]=[C:12]([CH:30]=[CH:31][CH:32]=1)[CH2:13][NH:14][CH2:15][CH2:16][C:17]([NH:19][C:20]1[CH:21]=[C:22]2[C:26](=[CH:27][CH:28]=1)[N:25]([CH3:29])[CH2:24][CH2:23]2)=[O:18])[C:4]1[S:5][CH:6]=[CH:7][CH:8]=1.C(Br)[C:34]1[CH:39]=[CH:38][CH:37]=[CH:36][CH:35]=1>>[ClH:1].[NH2:2][C:3](=[N:9][C:10]1[CH:11]=[C:12]([CH:30]=[CH:31][CH:32]=1)[CH2:13][NH:14][CH2:15][CH2:16][C:17]([NH:19][C:20]1[CH:21]=[C:22]2[C:26](=[CH:27][CH:28]=1)[N:25]([CH2:29][C:34]1[CH:39]=[CH:38][CH:37]=[CH:36][CH:35]=1)[CH2:24][CH2:23]2)=[O:18])[C:4]1[S:5][CH:6]=[CH:7][CH:8]=1

Participants

3

Reactant 2

HCID 7498Benzyl BromideHCID 18765813HCID 18765813, compound

Product 1

HCID 18765779HCID 18765779, compound

Procedure

The experimental protocol used is the same as that described for compound 54, with benzyl bromide replacing iodomethane. A white solid is obtained. Melting point: 193-195° C.

Workup

  1. customA white solid is obtained

Sources & evidence

ORD record
ord-1220c5d79ac14092aa5d1187ac9be70a
Source dataset
uspto-grants-2009_08
Patent number
US07576241B2

Reaction notes

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