HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-2-nitroaniline → HCID 22934712, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-2-nitroaniline | HCID 6979 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Methyl chloroglyoxylate | HCID 79846 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 22934712 | HCID 22934712 | — |
Reaction Steps
In a manner similar to that described in Referential Example 242, 4-chloro-2-nitroaniline was condensed with methyl chlorooxoacetate. In a manner similar to that described in Referential Example 266, the condensed compound was hydrolyzed. The residue was dissolved in methanol, 1N aqueous sodium hydroxide was added thereto, and the precipitated material was recoverd by filtration, whereby the title compound was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07576135B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-002956499cd447c5a7d6d905badbcea8 |
| Source note | uspto-grants-2009_08 |