HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 69253307, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | HCID 67056702 | HCID 67056702 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 69253307 | HCID 69253307 | 94.8% |
Reaction Steps
The compound (1.20 g) obtained in Example 51 was dissolved in tetrahydrofuran (32 mL), and lithium hydroxide (60.8 mg) and water (4 mL) were successively added under ice cooling, followed by stirring at room temperature for 14 hours. The solvent was distilled away under reduced pressure to give the title compound (1.12 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07576135B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-1275c4ac512a4746a96dadd9a84f8136 |
| Source note | uspto-grants-2009_08 |