Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2104524Generated: October 31, 2026

Diethylamine → HCID 66914259, compound

https://huagongshe.com/reaction/2104524

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiethylamineHCID 8021—
ReactantHCID 66913777HCID 66913777—
SolventDichloromethaneHCID 6344—
ProductHCID 66914259HCID 6691425987.9%

Reaction Steps

A solution of {4-[3-(4-chloromethyl-benzyloxy)-phenyl]-8-trifluoromethyl-quinolin-3-yl}phenyl-methanone (011 g, 0.2 mmol) and diethylamine(0.3 g, 5.7 mmol) in CH2Cl2 (5 ml) was stirred at r.t. After 24 hr, the reaction was concentrated and purified by column chromatography (eluent 25% EtOAc/Hex) to give the title compound as a foam (0.10 g); MS m/z 569.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07576215B2
Source datasetuspto-grants-2009_08
ORD IDord-7c1290aeece4486bb88a06a25325854c
Source noteuspto-grants-2009_08