HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → HCID 66914259, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | HCID 66913777 | HCID 66913777 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 66914259 | HCID 66914259 | 87.9% |
Reaction Steps
A solution of {4-[3-(4-chloromethyl-benzyloxy)-phenyl]-8-trifluoromethyl-quinolin-3-yl}phenyl-methanone (011 g, 0.2 mmol) and diethylamine(0.3 g, 5.7 mmol) in CH2Cl2 (5 ml) was stirred at r.t. After 24 hr, the reaction was concentrated and purified by column chromatography (eluent 25% EtOAc/Hex) to give the title compound as a foam (0.10 g); MS m/z 569.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07576215B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-7c1290aeece4486bb88a06a25325854c |
| Source note | uspto-grants-2009_08 |