HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methyl-3-phenyl-1H-1,2,4-triazole → HCID 68814737, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methyl-3-phenyl-1H-1,2,4-triazole | HCID 10877408 | — |
| Reactant | 4-Chloro-2-fluoro-5-methoxybenzaldehyde | HCID 14928268 | — |
| Reactant | (3-ethylphenyl)(2-methyl-5-phenyl-2H-1,2,4-triazol-3-yl)methanol | HCID 57803786 | — |
| Product | HCID 68814737 | HCID 68814737 | 67.6% |
Reaction Steps
According to the procedure for Intermediate 370.2, 1-methyl-3-phenyl-1H-1,2,4-triazole (65 mg, 0.40 mmol) and Intermediate 392.1 (80 mg, 0.45 mmol) afforded 94 mg of Intermediate 392.2 as a white solid. LCMS 348.25 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07576098B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-84dcd4a8e2a742a1b7f644c71458170e |
| Source note | uspto-grants-2009_08 |